Page 178 - Book Hosokawa Nanoparticle Technology Handbook
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FUNDAMENTALS                CH. 3 CHARACTERISTICS AND BEHAVIOR OF NANOPARTICLES AND ITS DISPERSION SYSTEMS












































                  Figure 3.5.26
                  Measuring method of angle of repose.



                  Rumpf’s model equation shows the relation between  load, (4) measure the shear force at the collapse point.
                  adhesion force F of the particles and tensile strength  The shearing strength of the powder bed   can be cal-
                               T
                    of the powder bed [6]                        culated as the value which divides the shear force by
                   T
                                                                 the fracture surface. Fig. 3.5.29 shows the schematic
                                                                 diagram of Jenike’s shear cell which is the ISO stan-
                               1      F   1     F
                                   N  c  T      T      (3.5.62)  dard [8]. Hirota et al. [9] invented the parallel plate-
                            T
                                      D p 2     D p 2            type shear tester which test powder shears between two
                                                                 parallel plates. The shearing strength for various nor-
                                                                 mal stresses concerning the same pre-consolidation
                  where N is the number of contact points on a particle  pressure is calculated, and the data are plotted on the
                         c
                  called coordination number and  Dp is the particle  stress plane like Fig. 3.5.29. The curved line which ties
                  size. Using Rumpf’s equation, the adhesion force F T  these plotting is called Powder Yield Locus (or PYL).
                  at a contact point in the powder bed can be calculated  The powder showing the linear relationship is called
                  from the tensile strength   of the powder bed.   the Coulomb powder. The tilt angle and the slope of the
                                       T
                                                                 straight line are called the angle of internal friction and
                  d) Shear test
                                                                 the internal friction factor, respectively. These values
                  As shown in Fig. 3.5.28, the procedure of shear test [7]  are used as flowability index of powder.
                  is as follows; (1) pack the powder in the shear cell,
                  (2) pre-consolidate and pre-shear the packed bed,

                  (3) acting the shear force on the upper cell under normal  	           	   tan  i     	  C  (3.5.63)
                                                                                  C
                                                                              i
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