Page 258 - Book Hosokawa Nanoparticle Technology Handbook
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4.5 STRUCTURE CONTROL OF NANOPARTICLE COLLECTIVES BY SINTERING AND BONDING   FUNDAMENTALS
                  4.5.4 Joining by FSW                           Only the probe is forced into the material during weld-
                                                                 ing, and the tool is moved along the interface. The
                    4.5.4.1 Friction stir welding                material is restricted to the back plate. The joining is
                  Friction stir welding (FSW) has already entered the  performed by plastic flow caused by the tool in the
                  practical use stage in various industrial fields such as  solid state. Because the peak temperature does not
                  railroad vehicles, vessels, structures, and cars [1–5],  reach the melting point and the material is in the solid
                  after it was developed by  TWI (British  Welding  state at this time, the grains are refined, the decrease in
                  Institute) in 1991 [6, 7]. Research and development in  the strength by welding is much lower than that of
                  this area has significantly increased in every country  fusion welding, and, in some cases, the strength of the
                  around the world. In this joining method, as shown in  joints is higher than that of the base metal. The details
                  Fig. 4.5.19(a), the columnar rotating tool at a high  of the tool are to be referred to a textbook on FSW [8].
                  speed contacts the materials to produce frictional heat,  A schematic diagram of the cross-sectional
                  and the materials can then be joined using the fric-  microstructure of the welded part is shown in
                  tional heat. As shown in Fig. 4.5.19(b), the tool con-  Fig. 4.5.20. The center, called the stir zone, consists of
                  sists of a large shoulder part and a probe part at the tip.  a recrystallized microstructure which consists of
                                                                 equiaxial grains of hundreds of nanometers to several
                                                                 micrometers in diameters. Figure 4.5.21 [9] shows
                    (a)                     (b)    ∅15
                                                                 TEM images of the stir zones of pure aluminum and
                                                                 pure Fe (IF steel). Outside the stir zone, there is the
                     Retreating     Welding direction
                       Side                                      thermo-mechanically affected zone (TMAZ), in which
                                                                 the crystal grain was extended by plastic modification.
                                                                 Outside the  TMAZ, the heat affected zone (HAZ)
                                            Sho    ulder
                                                         Probe
                                                                 exists, which is affected by the heat, but not affected
                                      Advancing                  by the plastic deformation. As a reference, for the nor-
                                        side       M6
                                                                 mal fusion welding, the grains grow from several tens
                                                                 of microns to several hundreds of microns.
                  Figure 4.5.19                                   According to Frigaard et al. [10], the heat input dur-
                  Friction stir welding and tool (example for 5-mm thick plate).
                                                                 ing FSW, Q(W), can be expressed as follows:
                                                                                    4
                                                                                Q       PNR 3          (4.5.1)
                                                                                       2
                                                                                    3
                    Base metal      Stir zone
                                                                 where    is the friction coefficient,  P the pressure
                                                                     3
                                                                 (N/m ),  N the tool rotation speed (/s), and  R the
                                                                 shoulder diameter (m). For this equation, it is
                       HAZ                  TMAZ                 assumed that the heat is generated only between the
                                                                 shoulder of the tool and the material. P is the load per
                  Figure 4.5.20                                  unit area of the shoulder part. Equation (4.5.1) can be
                  Schematic illustration of microstructure.      used when the tool is not moved. When the tool is




















                  Figure 4.5.21
                  Recrystallized microstructure in stir zone of pure Al and IF steel.

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