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166   SILICON MICROMACHINING:  SURFACE

      6.6  PROCESSES     USING    BOTH   BULK    AND SURFACE
          MICROMACHINING

      It is clearly possible to fabricate  a variety of microsensor and MEMS  devices using  either
      solely  bulk-micromachining  techniques  or  surface-micromachining  techniques.  Some  of
     these  devices  have  been  described  here  via  worked  examples,  and a  large  number  other
     devices have been  described  in the literature (Gardner  1994).
        However,  all  such  devices  suffer  from  limitations  that  are  inherent  in one  or  the  other
     of these  two techniques.  Taking  advantages  of the fabrication  possibilities  offered by bulk-
     and  surface-micromachining  techniques  and combining  the  two  techniques  in  fabricating
     MEMS   devices opens up  new opportunities  for  the  fabrication  of a  new class of  MEMS
     devices  that  are  not  possible  to  fabricate  using  either  of  the  technique  alone.  Several
     devices  have  been  fabricated  using  a  combination  of  bulk-  and  surface-micromachining
     processes. Two of these devices are now described  in the Worked  Examples 6.9 and  6.10.


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        Worked  Example  E6.9:  Micronozzles
        Objective:
        Micronozzles  are  important  in  a  variety  of  optical  instruments  and  micromechanical
        devices,  for  example,  beam-defining elements,  high-resolution  ink-jet  printing  heads,
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        microvalves,  and  flow  controllers .  The  objective  in  this  example  is  to  fabricate  a
        silicon  nitride  nozzle with a submicron  aperture.

        Process Flow:
        The  process  flow  used in micromachining the micronozzle is depicted  in Figure  6.20.

        1.  The  fabrication  process  starts  with  a  lightly  doped  (100)  Si  wafer  onto  which  a
          composite  layer  of  SisN 4  and  SiO 2,  160 nm  and  500  nm  thick,  respectively,  is
          deposited.  The  nitride  and  oxide  are  then  plasma-etched  to  form  a  circular 3 \im-
          diameter  mask  (Figure  6.20(a)).
        2.  Using this mask, the Si is dry-etched  to form the Si moulds for the nozzle. The plasma
          etch is chosen such that the etch is semianisotropic  for an etch depth of approximately
          3.5 nm  and  a  sideways  undercutting of  approximately 5 nm  (Figure 6.20(b)).  The
          oxide  mask is first etched  in an HF solution and then the nitride mask is removed by
          further  etching Si  in  a  wet  isotropic etch that fully  undercuts the  nitride mask.
        3.  The  next  step is to coat the  Si moulds in Si 3N 4 to form  the nozzles. A thin (few tens
          of  nanometers) layer  of  padding  SiO 2  is  deposited,  followed  by  LPCVD  of  about
          350 to 550 nm of Si 3N 4.  The deposited  layers are highly conformal, replicating even
          the  high-cusped moulds (Figure 6.20(c)).  A  second  layer  of  SiC»2  is  deposited  over
          the  nitride. This layer serves as a protective layer for the fine mould tips.
        4.  To  define  the  nozzle  aperture,  Si 3N 4  has  to  be  etched  back  to  expose  the required
          portion  of  the  Si  mould.  This  is  accomplished  by  coating  the  surface  with  a thick

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       For details, see Farooqui  and Evans (1992).
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       Commercial  applications  of  microstructures  are  presented  in Chapter  1.
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